On the measurement of PANs by gas chromatography and electron capture detection

Frank M. Flocke, Andrew J. Weinheimer, Aaron L. Swanson, James M. Roberts, Rainer Schmitt, Stephen Shertz

Research output: Contribution to journalArticlepeer-review

60 Scopus citations

Abstract

A fast, automated, gas chromatographic system for the airborne measurement of PAN and a series of its homologues is described and its performance is evaluated. Response factors for PAN, PPN, APAN, PiBN, and MPAN have been determined and are discussed with regard to ECD response and to potential losses in the analytical system. Calibration methods used for these tasks are described and compared. The results from this work should help investigators who are employing the widely used GC/ECD method for the measurement of peroxyacyl nitrates to evaluate peaks of PAN homologues that cannot be calibrated for by using the reported response factors.

Original languageEnglish
Pages (from-to)19-43
Number of pages25
JournalJournal of Atmospheric Chemistry
Volume52
Issue number1
DOIs
StatePublished - Sep 2005

Keywords

  • Air pollution
  • Atmospheric chemistry
  • Gas chromatography
  • Peroxyacetyl nitrate
  • Peroxyacyl nitrates

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